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《江苏农业科学》[ISSN:1002-1302/CN:32-1214/S]

卷:

第48卷

期数:

2020年第2期

页码:

57-64

栏目:

专论与综述

出版日期:

2020-03-05

文章信息/Info

Title:

Detection of veterinary drug residues in animal origin agro-products based on liquid chromatography tandem high resolution mass spectrometry (LC-HRMS)：a review

作者:

王卉; 刘庆菊; 韩平

1.北京农业质量标准与检测技术研究中心，北京 100097； 2.农业农村部农产品质量安全风险评估实验室(北京)，北京 100097；
3.农产品产地环境监测北京市重点实验室，北京 100097

Author(s):

Wang Hui; et al

关键词:

液相色谱（LC）-高分辨质谱（HRMS）; 动物源农产品; 兽药残留; 样品前处理; 色谱分离; 质谱检测; 数据处理

Keywords:

-

分类号:

TS207.5⁺3

DOI:

-

文献标志码:

A

摘要:

液相色谱-高分辨质谱（LC-HRMS）具有高分辨率、高通量、高精确度等优势，在动物源农产品的兽药残留检测研究中显示出极大的潜力。本文综述了2014—2018年LC-HRMS检测动物源农产品中兽药残留的应用研究进展。其中，QuEChERS方法和有机溶剂提取法是常用的兽药残留提取方法，提取液用PSA、C₁₈和氧化铝等吸附剂净化，绿色的样品前处理方法是未来的发展趋势；液相系统和色谱柱的改良，使兽药化合物得到更好的分离，提高了质谱检测的灵敏度；HRMS分辨率和灵敏度的提高，增强了LC-HRMS定性定量分析动物源农产品中兽药残留的能力；数据处理软件的开发和应用，提高了LC-HRMS在兽药残留检测中的工作效率。尽管LC-HRMS在兽药残留检测中取得了进展，但仍存在不足和发展空间。

Abstract:

-

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相似文献/References:

备注/Memo

备注/Memo:

收稿日期：2018-11-08
基金项目：农业农村部农产品质量安全风险评估实验室(北京)开放课题(编号：kfkt201703)；北京市农林科学院青年基金项目(编号：QNJJ201833)。
作者简介：王卉(1982—)，女，内蒙古鄂伦春人，博士，助理研究员，主要从事农产品安全检测工作。E-mail：wangh@brcast.org.cn。
通信作者：韩平，副研究员，主要从事农产品安全检测工作。E-mail：hanp@brcast.org.cn。

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更新日期/Last Update: 2020-01-20