|本期目录/Table of Contents|

[1]吴东明,邓晓,李怡,等.土壤溶解性有机质的提取与特性分析研究进展[J].江苏农业科学,2019,47(03):6-11.
　Wu Dongming,et al.Research progress for extraction and characterization of dissolved organic matter in soil[J].Jiangsu Agricultural Sciences,2019,47(03):6-11.
点击复制

土壤溶解性有机质的提取与特性分析研究进展(PDF)
分享到：

《江苏农业科学》[ISSN:1002-1302/CN:32-1214/S]

卷:
第47卷
期数:
2019年第03期
页码:
6-11
栏目:
专论与综述
出版日期:
2019-02-02

文章信息/Info

Title:
Research progress for extraction and characterization of dissolved organic matter in soil
作者:
吴东明1; 2;  邓晓1; 2;  李怡1; 2;  陈耀华3;  武春媛1; 2
1.中国热带农业科学院环境与植物保护研究所，海南海口 570100； 2.农业部儋州农业环境科学观测实验站，海南儋州 571737；
3.海南省农业信贷担保有限责任公司，海南海口 570105
Author(s):
Wu Dongming; et al
关键词:
土壤溶解性有机质; 提取; 表征; 化学性质; 物质组成
Keywords:
-
分类号:
S153.6
DOI:
-
文献标志码:
A
摘要:
溶解性有机质(DOM)在土壤中具有重要的生态环境意义，对DOM的正确提取、表征是认识DOM生态环境意义的重要基础。因此，本文介绍了水提法、盐提法、酸提法、碱提法提取土壤DOM的优缺点，分析了离子类型、离子浓度、pH值、浸提时间与温度、水土比、土壤含水量等因素对DOM提取效率和物质组成的影响。综述了元素分析技术、光谱技术、色谱技术、质谱技术、电化学技术、显微镜技术在DOM极性、分子量、疏水性、芳香性、官能团、氧化还原性、物质组成、微观形态等方面的表征应用及优缺点，并指出了将土壤DOM提取技术与表征技术有机统一起来，大力发展新技术、原位表征技术、多技术联用以及技术与数学模型、计量化学联用是增强对土壤DOM认识的重要发展方向。
Abstract:
-

参考文献/References:

［1］Zsolnay A. Dissolved organic matter：artefacts，definitions，and functions［J］. Geoderma，2003，113(3/4)：187-209.
［2］凌婉婷，徐建民，高彦征，等. 溶解性有机质对土壤中有机污染物环境行为的影响［J］. 应用生态学报，2004，15(2)：326-330.
［3］Herbert B E，Bertsch P M，Mcfee W W，et al. Characterization of dissolved and colloidal organic matter in soil solution：a review［J］. Carbon Forms & Functions in Forest Soils，1995(2)：63-88.
［4］Kalbitz K，Solinger S，Park J H，et al. Controls on the dynamics of dissolved organic matter in soils：a review［J］. Soil Science，2000，165(4)：277-304.
［5］Bolan N S，Adriano D C，Kunhikrishnan A，et al. Dissolved organic matter：biogeochemistry，dynamics，and environmental significance in soils［J］. Advances in Agronomy，2011，110：1-75.
［6］闰金龙，江韬，赵秀兰，等. 含生物质炭城市污泥堆肥中溶解性有机质的光谱特征［J］. 中国环境科学，2014，34(2)：459-465.
［7］Chantigny M H，Harrison-Kirk T，Curtin D，et al. Temperature and duration of extraction affect the biochemical composition of soil water-extractable organic matter［J］. Soil Biology and Biochemistry，2014，75：161-166.
［8］Hu S H，Wu Y G，Yi N，et al. Chemical properties of dissolved organic matter derived from sugarcane rind and the impacts on copper adsorption onto red soil［J］. Environmental Science & Pollution Research，2017，24(26)：1-11.
［9］谢理，杨浩，渠晓霞，等. 滇池典型陆生和水生植物溶解性有机质组分的光谱分析［J］. 环境科学研究，2013，26(1)：72-79.
［10］Minor E C，Swenson M M，Mattson B M，et al. Structural characterization of dissolved organic matter：a review of current techniques for isolation and analysis［J］. Environmental Science Processes & Impacts，2014，16(9)：2064-2079.
［11］何伟，白泽琳，李一龙，等. 溶解性有机质特性分析与来源解析的研究进展［J］. 环境科学学报，2016，36(2)：359-372.
［12］McAdams B C，Aiken G R，McKnight D M，et al. High pressure size exclusion chromatography (HPSEC) determination of dissolved organic matter molecular weight revisited：accounting for changes in stationary phases，analytical standards，and isolation methods［J］. Environmental science & technology，2017，52(2)：722-730.
［13］Poulin B A，Ryan J N，Aiken G R. Effects of iron on optical properties of dissolved organic matter［J］. Environmental Science & Technology，2014，48(17)：10098-10106.
［14］Rennert T，Kai F G，Mansfeldt T. Extraction of water-soluble organic matter from mineral horizons of forest soils［J］. Journal of Plant Nutrition and Soil Science，2007，170(4)：514-521.
［15］Zheng X D，Chen X B，Liang C M. Influence of extractants and filter materials in the extraction of dissolved organic matter (DOM) from subtropical agricultural soil［J］. 2018，30(3)：165-172.
［16］Provenzano M R，Caricasole P，Brunetti G，et al. Dissolved organic matter extracted with water and a saline solution from different soil profiles［J］. Soil Science，2010，175(6)：255-262.
［17］Courdouan A，Christl I，Meylan S，et al. Isolation and characterization of dissolved organic matter from the Callovo-Oxfordian formation［J］. Applied Geochemistry，2007，22(7)：1537-1548.
［18］王贵胤，张世熔，周玲，等. 不同试剂提取紫色土溶解性有机碳含量研究［J］. 西南农业学报，2012，25(6)：2184-2189.
［19］李忠佩，焦坤，吴大付. 不同提取条件下红壤水稻土溶解有机碳的含量变化［J］. 土壤，2005，37(5)：512-516.
［20］Jones D L，Willett V B. Experimental evaluation of methods to quantify dissolved organic nitrogen (DON) and dissolved organic carbon (DOC) in soil［J］. Soil Biology & Biochemistry，2006，38(5)：991-999.
［21］Bolan N S，Baskaran S，Thiagarajan S. An evaluation of the methods of measurement of dissolved organic carbon in soils，manures，sludges，and stream water［J］. Communications in Soil Science & Plant Analysis，2008，27(13/14)：2723-2737.
［22］Takács M，Füleky G. Characterization of dissolved organic matter (DOM) extracted from soils by hot water percolation (HWP)［J］. Agrokémia s Talajtan，2010，59(1)：99-108.
［23］张甲珅，陶澍，曹军. 土壤中水溶性有机碳测定中的样品保存与前处理方法［J］. 土壤通报，2000，31(4)：174-176.
［24］Yuan D H，Zhou Q，An Y C，et al. Impacts of soil improvement on the pollutant-removal performance and DOM characteristics using a simulation experiment［J］. Ecological Indicators，2018(5)：1-10.
［25］Mostofa K M G，Li L，Liu C. Detection of tyrosine，trace metals and nutrients in cow dung：the environmental significance in soil and water environments［J］. Acta Geochimica，2018，37(4)：632-638.
［26］Li Q，Guo X J，Chen L，et al. Investigating the spectral characteristic and humification degree of dissolved organic matter in saline-alkali soil using spectroscopic techniques［J］. Frontiers of Earth Science，2017，11(1)：76-84.
［27］许伟. 水溶性有机物的电子转移能力及其对微生物异化铁还原影响的研究［D］. 成都：四川师范大学，2009.
［28］Cao X，Aiken G R，Butler K，et al. Comparison of the chemical composition of dissolved organic matter in three lakes in Minnesota，USA［J］. Environmental Science & Technology，2018，52(4)：1747-1755.
［29］Yu M，He X，Liu J，et al. Characterization of isolated fractions of dissolved organic matter derived from municipal solid waste compost［J］. Science of the Total Environment，2018，635(9)：275-283.
［30］Xie W M，Zhang S S，Ruan L，et al. Evaluating soil dissolved organic matter extraction using three-dimensional excitation-emission matrix fluorescence spectroscopy［J］. Pedosphere，2017，27(5)：968-973.
［31］Philibert M，Rosario-Ortiz F，Suffet M. Comparison of two polarity measurements of hydrophobic organic matter for the evaluation of water treatment processes：XAD resin and PRAM［J］. Water Science & Technology，2012，66(11)：2418-2424.
［32］Namjesnik-Dejanovic K，Cabaniss S E. Reverse-phase HPLC method for measuring polarity distributions of natural organic matter［J］. Environmental Science & Technology，2004，38(4)：1108-1114.
［33］郭瑾，马军. 天然有机物提取及表征技术近期发展动态［J］. 现代化工，2007，27(2)：12-16.
［34］李帅东，张明礼，杨浩，等. 昆明松华坝库区表层土壤溶解性有机质(DOM)的光谱特性［J］. 光谱学与光谱分析，2017，37(4)：1183-1188.
［35］Wu D M，Yun Y H，Jiang L，et al. Influence of dissolved organic matter on sorption and desorption of MCPA in ferralsol［J］. Science of the Total Environment，2018，616：1449-1456.
［36］Wang Y L，Yang C M，Li J H，et al. The chemical composition and source identification of soil dissolved organic matter in riparian buffer zones from Chongming Island，China［J］. Chemosphere，2014，111(9)：505-512.
［37］Wang C K，Zhang X J，Wang J，et al. Characterization of dissolved organic matter as N-nitrosamine precursors based on hydrophobicity，molecular weight and fluorescence［J］. Journal of Environmental Sciences，2013，25(1)：85-95.
［38］Baluha D R，Blough N V，Del V R. Selective mass labeling for linking the optical properties of chromophoric dissolved organic matter to structure and composition via ultrahigh resolution electrospray ionization mass spectrometry［J］. Environmental Science & Technology，2013，47(17)：9891-9897.
［39］Wickramasekara S，Hernández-Ruiz S，Abrell L，et al. Natural dissolved organic matter affects electrospray ionization during analysis of emerging contaminants by mass spectrometry［J］. Analytica Chimica Acta，2012，717(5)：77-84.
［40］Bi R，Lu Q，Yu W，et al. Electron transfer capacity of soil dissolved organic matter and its potential impact on soil respiration［J］. Journal of Soils & Sediments，2013，13(9)：1553-1560.
［41］Yuan T，Yuan Y，Zhou S G，et al. A rapid and simple electrochemical method for evaluating the electron transfer capacities of dissolved organic matter［J］. Journal of Soils & Sediments，2011，11(3)：467-473.
［42］陶亚. 水溶性有机物的电子转移能力及其构效关系的研究［D］. 长沙：湖南农业大学，2012.
［43］He X S，Xi B D，Cui D Y，et al. Influence of chemical and structural evolution of dissolved organic matter on electron transfer capacity during composting［J］. Journal of Hazardous Materials，2014，268(3)：256-263.
［44］毕冉，周顺桂，袁田，等. 水溶性有机物电子转移能力及其生态效应［J］. 生态学报，2013，33(1)：45-52.
［45］Yu J，Xu Q，Liu Z，et al. Morphological characteristics of fulvic acid fractions observed by atomic force microscopy［J］. Journal of Microscopy，2013，252(1)：71-78.
［46］Alivio T E G，Fleer N A，Singh J，et al. Stabilization of Ag-Au bimetallic nanocrystals in aquatic environments mediated by dissolved organic matter：a mechanistic perspective［J］. Environmental Science & Technology，2018，52(13)：7269-7278.

相似文献/References:

[1]袁竹连.番木瓜叶叶绿素的提取及叶绿素铜钠的制备[J].江苏农业科学,2013,41(04):244.
[2]郑蔚然,胡莉,袁玉伟,等.蓝莓中花青素提取及检测技术的研究进展[J].江苏农业科学,2013,41(06):233.
　Zheng Weiran,et al.Research progress on extraction and detection technology for anthocyanin in blueberries[J].Jiangsu Agricultural Sciences,2013,41(03):233.
[3]张宏喜,周婷婷,李楠,等.利用乙醇自催化法提取棉秆中的木质素[J].江苏农业科学,2013,41(06):243.
　Zhang Hongxi,et al.Extraction of lignin from cotton stalks by pulping autocatalytic method of ethanol[J].Jiangsu Agricultural Sciences,2013,41(03):243.
[4]郭志欣,顾地周,宋宇辉,等.五味子药渣中多糖提取工艺研究[J].江苏农业科学,2013,41(05):254.
　Guo Zhixin,et al.Study on extraction technology of polysaccharide from dregs of Schisandra chinensis (Turcz.) Bailey[J].Jiangsu Agricultural Sciences,2013,41(03):254.
[5]朱月,段蕊晔,毕晓丹.杏鲍菇多糖提取条件研究[J].江苏农业科学,2013,41(05):276.
　Zhu Yue,et al.Research on extraction conditions of polysaccharide from [WTBX]Pleurotus eryngii[WTBZ][J].Jiangsu Agricultural Sciences,2013,41(03):276.
[6]孙仓,李长权.稠李果实中原花青素的提取工艺[J].江苏农业科学,2013,41(05):279.
　Sun Cang,et al.Extraction technology of proanthocyanidin from fruits of [WTBX]Prunus padus[WTBZ] L.[J].Jiangsu Agricultural Sciences,2013,41(03):279.
[7]孔庆新,李思阳,刘凯,等.荔枝草中高车前苷的提取与分析[J].江苏农业科学,2014,42(12):304.
　Kong Qingxin,et al.Extraction and analysis of homoplantaginin from Salvia plebeia[J].Jiangsu Agricultural Sciences,2014,42(03):304.
[8]李栎,纪春艳,王振中.水稻叶片质膜蛋白的提取与纯化[J].江苏农业科学,2013,41(06):44.
　Li Li,et al.Separation and purification of plasma membrane proteins from rice leaves[J].Jiangsu Agricultural Sciences,2013,41(03):44.
[9]邓艳美,王红妹,万从庆.青花菜中硫代葡萄糖苷的提取工艺[J].江苏农业科学,2013,41(06):254.
　Deng Yanmei,et al.Extraction technology of glucosinolates from broccoli[J].Jiangsu Agricultural Sciences,2013,41(03):254.
[10]翁艳英,谭义秋,韦藤幼,等.减压内部沸腾法提取绞股蓝总皂苷的工艺[J].江苏农业科学,2014,42(10):249.
　Wen Yanying,et al.Extraction process of total saponins from Gynostemma pentaphyllum by internal pressure boiling method[J].Jiangsu Agricultural Sciences,2014,42(03):249.

备注/Memo

备注/Memo:
收稿日期：2018-09-21
基金项目：海南省重大科技计划(编号：ZDKJ2017002)；中国热带农业科学院环境与植物保护研究所自主选题项目(编号：hzsjy2018004)；国家自然科学基金(编号：41371465)。
作者简介：吴东明(1991—)，男，广东湛江人，硕士，研究实习员，从事土壤有机化学与污染物环境行为研究。E-mail：wudomy@126.com。
通信作者：武春媛，博士，研究员，从事土壤有机污染控制研究。E-mail：cywu@catas.cn。
更新日期/Last Update: 2019-02-05