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《江苏农业科学》[ISSN:1002-1302/CN:32-1214/S]

卷:

第41卷

期数:

2013年10期

页码:

251-253

栏目:

质量安全与检测分析

出版日期:

2013-10-25

文章信息/Info

Title:

Improvement of detection method for pyrethroid pesticide in codfish

作者:

曹军¹; 黄月芳²; 沈山江¹

1.江苏省盐城出入境检验检疫局，江苏盐城 224002； 2.江苏省盐城市盐都区农业委员会，江苏盐城 224002

Author(s):

Cao Jun; et al

关键词:

分散固相萃取; QuEChERS; 鳕鱼; 菊酯类农药

Keywords:

-

分类号:

S481+.8

DOI:

-

文献标志码:

A

摘要:

建立了鳕鱼中菊酯类农药多残留的简单、快速检测方法。采用乙腈缓冲溶液进行提取，改进的QuEChERS法进行分散固相萃取净化，结合气相色谱法对鳕鱼中6种菊酯类农药同时检测，取得了满意结果。添加样品的回收率为82.9%～105.8%，相对标准偏差在2.8%～7.1%，方法最低检出限分别是氯氰菊酯为0.02 mg/kg，甲氰菊酯、联苯菊酯、高效氯氟氰菊酯、溴氰菊酯、氰戊菊酯均为0.01 mg/kg。

Abstract:

-

参考文献/References:

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备注/Memo

备注/Memo:

收稿日期：2013-03-18
作者简介：曹军（1982—），男，安徽怀宁人，硕士，工程师，主要从事农产品及环境分析。E-mail:cj925928@126.com。

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更新日期/Last Update: 2013-10-25