|本期目录/Table of Contents|

[1]黄雪玲,戚隽渊,魏厚道,等.固相萃取-高效液相色谱法同时测定水产品中的己烯雌酚和甲基睾丸酮[J].江苏农业科学,2015,43(05):285-287.
　Huang Xueling,et al.Simultaneous determination of diethylstilbestrol and methyltestosterone in aquatic products by solid phase extraction-high performance liquid chromatography[J].Jiangsu Agricultural Sciences,2015,43(05):285-287.
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固相萃取-高效液相色谱法同时测定水产品中的己烯雌酚和甲基睾丸酮(PDF)
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《江苏农业科学》[ISSN:1002-1302/CN:32-1214/S]

卷:
第43卷
期数:
2015年05期
页码:
285-287
栏目:
质量安全与检测分析
出版日期:
2015-05-25

文章信息/Info

Title:
Simultaneous determination of diethylstilbestrol and methyltestosterone in aquatic products by solid phase extraction-high performance liquid chromatography
作者:
黄雪玲1;  戚隽渊1;  魏厚道2;  郭霞1;  孙建华1;  刘琴1;  丁义1
1.上海市水产研究所，上海 200433； 2.上海天复检测技术有限公司，上海 200125
Author(s):
Huang Xueling; et al
关键词:
固相萃取; 液相色谱; 己烯雌酚; 甲基睾丸酮
Keywords:
-
分类号:
O657.7+2
DOI:
-
文献标志码:
A
摘要:
建立了SPE-HPLC同时测定水产品中己烯雌酚和甲基睾丸酮的方法。样品经乙酸乙酯超声提取，正己烷脱脂，过C18型固相萃取柱净化，以甲醇-0.5%甲酸(70 ∶30)为流动相，检测波长254 nm，外标法定量。相对标准偏差为3.5%~5.6%，己烯雌酚、甲基睾丸酮的检出限分别为5.0、6.0 μg/kg。加标回收率在78%~93%之间。
Abstract:
-

参考文献/References:

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备注/Memo

备注/Memo:
收稿日期：2014-08-28
作者简介：黄雪玲(1981—)，女，河南周口人，硕士，助理工程师，主要从事水产品药物残留检测技术研究。Tel：(021)65482263；E-mail：butterfly032008@163.com。
更新日期/Last Update: 2015-05-25