[1]乐渊,邓正敏,刘春华,等.多壁碳纳米管净化-超高效液相色谱串联质谱法测定香蕉中8种新烟碱类杀虫剂[J].江苏农业科学,2020,48(04):181-186.
　Le Yuan,et al.Determination of eight neonicotinoid insecticides residues in banana using ultra-performance liquid chromatography-tandem mass spectrometry coupled with multiwalled carbon nanotubes purification[J].Jiangsu Agricultural Sciences,2020,48(04):181-186.
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多壁碳纳米管净化-超高效液相色谱串联质谱法
测定香蕉中8种新烟碱类杀虫剂()

《江苏农业科学》[ISSN:1002-1302/CN:32-1214/S]

卷:
第48卷
期数:
2020年第04期
页码:
181-186
栏目:
贮藏加工与检测分析
出版日期:
2020-03-25

文章信息/Info

Title:
Determination of eight neonicotinoid insecticides residues in banana using ultra-performance liquid chromatography-tandem mass spectrometry coupled with multiwalled carbon nanotubes purification
作者:
乐渊;  邓正敏;  刘春华;  吴南村
中国热带农业科学院分析测试中心/海南省热带果蔬产品质量安全重点实验室，海南海口 571101
Author(s):
Le Yuan; et al
关键词:
香蕉; 新烟碱类杀虫剂; 多壁碳纳米管; 超高效液相色谱-串联质谱; 加标回收率; 残留量
Keywords:
-
分类号:
S481+.8
DOI:
-
文献标志码:
A
摘要:
建立基于多壁碳纳米管净化、超高效液相色谱串联质谱技术同时测定香蕉中呋虫胺等8种新烟碱类杀虫剂残留量的分析方法。香蕉样品中用含1%乙酸的乙腈提取后，经多壁碳纳米管净化后，用超高效液相色谱-串联质谱法测定。呋虫胺等8种新烟碱类杀虫剂的质量浓度在0.005~0.200 mg/L范围内线性良好，最低检出限在0.03～0.44 μg/kg 之间，相关系数均大于0.99，平均加标回收率在75.2%~114.9%之间，相对标准差在0.3%~9.5%之间。与N-丙基乙二胺和石墨化碳黑吸附剂相比，多壁碳纳米管具有净化效果好和效率高等优点。方法学考察及实际样品的测定证明该方法简便、快速、准确，可用于香蕉中呋虫胺等8种新烟碱类杀虫剂残留量的检测。
Abstract:
-

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备注/Memo

备注/Memo:
收稿日期：2018-11-22
基金项目：现代农业产业技术体系建设专项(编号：CARS-31-13)；热带农产品质量安全科技创新团队项目(编号：1630082017002)。
作者简介：乐渊(1985—)，男，江西抚州人，硕士，助理研究员，主要从事农产品质量安全研究。E-mail：leyuan06@sina.com。
更新日期/Last Update: 2020-02-20